1-Ethynyl-4-propoxybenzene → 1-Ethynyl-4-propylbenzene

HRID 493034Notes

Reaction equation

HRID 493034 reaction equation
C(OC(OC1C=C[C:12]([C:15]#[C:16][C:17]2[CH:22]=[CH:21][C:20](OCCC)=[CH:19][CH:18]=2)=CC=1)=O)(C)(C)C.[CH2:27](OC1C=CC(C#C)=CC=1)[CH2:28]C>>[CH2:16]([C:17]1[CH:18]=[CH:19][C:20]([C:27]#[CH:28])=[CH:21][CH:22]=1)[CH2:15][CH3:12]

Participants

3

Reactant 2

HCID 27751231-Ethynyl-4-propoxybenzeneHCID 22925937HCID 22925937, compound

Product 1

HCID 27751331-Ethynyl-4-propylbenzene

Procedure

1-[4-(tert-butoxycarbonyloxy)phenyl]-2-(4-n-propyloxyphenyl)acetylene was gained in the same manner as in the step (iii) of the Example 31, except for using 4-(n-propyloxy)phenylacetylene obtained in the step (iii) instead of 4-n-propylphenylacetylene.

Sources & evidence

ORD record
ord-7a9829db491640ae9ab748c4410da09c
Source dataset
uspto-grants-2009_05
Patent number
US07534547B2

Reaction notes

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