反应详情

1 g (4.73 mmol) of 4-nitrophthalic acid is dissolved in 10 mL of anhydrous ethanol. The solution is stirred at room temperature and degassed under argon. 50 mg of palladium/charcoal (5%) are added in a single portion and hydrogen is bubbled into the solution. After 3 hours, the solution is filtered through Celite and then evaporated.

1. customdegassed under argon
2. addition50 mg of palladium/charcoal (5%) are added in a single portion and hydrogen
3. customis bubbled into the solution
4. filtrationthe solution is filtered through Celite
5. customevaporated