Furfuryl Alcohol → HCID 22036385, compound

HRID 493256Notes

Reaction equation

HRID 493256 reaction equation
[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH2:6][OH:7].[Cl:8][C:9]1[C:14](Cl)=[N:13][CH:12]=[CH:11][N:10]=1>>[Cl:8][C:9]1[C:14]([O:7][CH2:6][C:2]2[O:1][CH:5]=[CH:4][CH:3]=2)=[N:13][CH:12]=[CH:11][N:10]=1

Participants

3

Reactant 2

HCID 7361Furfuryl AlcoholHCID 785752,3-Dichloropyrazine

Product 1

HCID 22036385HCID 22036385, compoundYield 68%

Procedure

The title compound was prepared according to the procedure described in Example 1, Step 1, starting from 2-furanmethanol (4.18 g, 42.7 mmol), 2,3-dichloropyrazine (2.05 g, 13.8 mmol) and KO-t-BuO (1.82 g, 16.2 mmol). The product, which was obtained as a yellowish oil in 68% yield, was used directly in the next step.

Workup

  1. customThe product, which was obtained as a yellowish oil in 68% yield

Sources & evidence

ORD record
ord-6a32b7327cd8442a9489a678e7cae8c6
Source dataset
uspto-grants-2009_05
Patent number
US07534794B2

Reaction notes

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