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HRID49359

反应详情

EQUATION

反应方程式

HRID 49359 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)[Si](C)(C)OCc1ccc(OCc2cc(C=O)cs2)cc1CO[Si](C)(C)C(C)(C)C
HCID20636303

未命名化合物

结构：CC[Mg]Br
HCID178418443

未命名化合物

PRODUCTS

生成物

1
结构：CCC(O)c1csc(COc2ccc(CO[Si](C)(C)C(C)(C)C)c(CO[Si](C)(C)C(C)(C)C)c2)c1
HCID69824620

未命名化合物

PROCEDURE

实验过程

In a manner similar to that of Example 9(a), by reaction of 33 g (65 mmol) of 5-[3,4-bis(tert-butyldimethylsilanyloxymethyl)phenoxymethyl]thiophene-3-carbaldehyde with 44 mL (130 mmol) of ethylmagnesium bromide, the product is obtained in the form of a yellow oil (m=28.4 g; Y=88%).

WORKUP

后处理

  1. customthe product is obtained in the form of a yellow oil (m=28.4 g; Y=88%)