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HRID49360

反应详情

EQUATION

反应方程式

HRID 49360 的结构方程式

REACTANTS

反应物

1
结构：CCC(O)c1csc(COc2ccc(CO[Si](C)(C)C(C)(C)C)c(CO[Si](C)(C)C(C)(C)C)c2)c1
HCID69824620

未命名化合物

PRODUCTS

生成物

1
结构：CCC(=O)c1csc(COc2ccc(CO[Si](C)(C)C(C)(C)C)c(CO[Si](C)(C)C(C)(C)C)c2)c1
HCID20636288

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：[Mn+4].[O-2].[O-2]
催化剂HCID178418406

未命名化合物

PROCEDURE

实验过程

In a manner similar to that of Example 9(b), by reaction of 28 g (52 mmol) of 1{5-[3,4-bis(tert-butyldimethylsilanyloxymethyl)phenoxymethyl]-3-thienyl}-1-propanol with 45 g (520 mmol) of manganese dioxide, the desired product is obtained in the form of an orange-coloured oil (m=26 g; Y=93%).