HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-bromo-N-quinolin-7-ylbenzamide → HCID 57682724, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-bromo-N-quinolin-7-ylbenzamide | HCID 831408 | — |
| Reactant | 5-Chloro-2-methoxyphenylboronic acid | HCID 2735751 | — |
| Product | HCID 57682724 | HCID 57682724 | — |
Reaction Steps
Using the procedure outlined in Example 58, the title compound was prepared from 4-bromo-N-quinolin-7-ylbenzamide (Example 82) (65 mg, 0.199 mmol) and 5-chloro-2-methoxyphenylboronic acid (42 mg, 0.22 mmol) as a colourless gum. 1H NMR (400 MHz, CDCl3) δ (ppm): 8.91 (dd, 1H), 8.18 (d, 1H), 8.13 (m, 3H), 7.98, (d, 2H), 7.86 (d, 1H), 7.66 (d, 2H), 7.36 (dd, 2H), 7.32 (m, 2H), 6.94 (d, 1H), 3.82 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07538121B2 |
| Source dataset | uspto-grants-2009_05 |
| ORD ID | ord-0252c05d399f4ccaba88df47adcce725 |
| Source note | uspto-grants-2009_05 |