HCID 68872644, compound → HCID 69268926, compound

HRID 494487Notes

Reaction equation

HRID 494487 reaction equation
[CH2:1]([C:5]([C:23]1[CH:28]=[CH:27][C:26]([F:29])=[CH:25][CH:24]=1)([CH2:19][CH2:20][CH2:21][CH3:22])[C:6]([CH:8](C(OCC)=O)[C:9]([O:11]CC)=O)=[O:7])[CH2:2][CH2:3][CH3:4].FC1C=CC(C(CCC)(CCC)C(C(C(OCC)=O)C(OCC)=O)=O)=CC=1>>[CH2:19]([C:5]1([CH2:1][CH2:2][CH2:3][CH3:4])[C:23]2[C:28](=[CH:27][C:26]([F:29])=[CH:25][CH:24]=2)[C:9]([OH:11])=[CH:8][C:6]1=[O:7])[CH2:20][CH2:21][CH3:22]

Participants

3

Reactant 2

HCID 68872644HCID 68872644, compoundHCID 68874303HCID 68874303, compound

Product 1

HCID 69268926HCID 69268926, compound

Procedure

The title compound was prepared according to the procedure of Example 14G, substituting the compound of Example 18E for the compound of Example 14F. 1H NMR (300 MHz, CDCl3): δ 0.52 (m, 2 H) 0.68 (t, J=7.35 Hz, 6 H) 0.88 (m, 2 H) 1.09 (m, 4 H) 1.82 (m, 2 H) 2.23 (m, 2 H) 6.17 (s, 1 H) 7.27 (m, 1 H) 7.42 (m, 1 H) 7.80 (dd, J=9.38, 2.76 Hz, 1H).

Sources & evidence

ORD record
ord-0a7731c48bd747319157175ab8a7d02b
Source dataset
uspto-grants-2009_05
Patent number
US07538105B2

Reaction notes

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