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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 494500Generated: October 30, 2026

HCID 68870329, compound → HCID 68871351, compound

https://huagongshe.com/reaction/494500

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 68870329HCID 68870329—
ReactantHCID 68871587HCID 68871587—
SolventEthanolHCID 702—
ProductHCID 68871351HCID 68871351—

Reaction Steps

The title compound was prepared according to the procedure of Example 22E, substituting the product of Example 23A, for the product of Example 22D. 1H NMR (300 MHz, CDCl3): δ 0.88 (m, 7 H) 1.06 (m, 1 H) 1.48 (m, 1 H) 1.55 (s, 3 H) 1.96 (m, 2 H) 3.76 (m, 2 H) 5.03 (m, 1 H) 5.83 (d, J=6.99 Hz, 1 H) 7.06 (m, 4 H) 7.29 (m, 5 H). Specific rotation: [α]D+12.4° (c 2.16, EtOH).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07538105B2
Source datasetuspto-grants-2009_05
ORD IDord-f7197be999d74ac4930fce3ab581c8d1
Source noteuspto-grants-2009_05