HCID 69267908, compound → HCID 68873333, compound

Participants

Reaction Steps

A solution of Example 35C (3.32 g, 9.47 mmol) in ethyl acetate (50 mL) was treated with 10% palladium on carbon (0.332 g, 10 weight percent) and stirred under a hydrogen balloon for 72 hours. The vessel was purged with nitrogen gas and the mixture was filtered through a pad of celite and the filtrate was concentrated in vacuo to give the title compound (2.48 g, 99%). 1H NMR (300 MHz, CDCl3): δ ppm 0.84 (m, 9 H) 1.19 (m, 6 H) 1.57 (m, 3H) 1.98 (m, 2 H) 7.34 (m, 5 H).

Provenance & Evidence