Sodium Hydroxide → HCID 68873352, compound

Participants

Reaction Conditions

Reaction Steps

A suspension of the product of Example 43H in water (3 mL) was treated with 0.997N sodium hydroxide solution (0.204 mL) and stirred at 25° C. for 1 hour. The solution was lyophilized to give 112 mg (84%) of a yellow solid. 1H NMR (300 MHz, DMSO-d6): δ ppm 0.49 (m, 1H) 0.66 (m, 6H) 0.92 (m, 2H) 1.11 (m, 2H) 1.38 (s, 3H) 1.72 (m, 1H) 2.14 (m, 1H) 2.96 (s, 3H) 7.33 (m, 3H) 7.45 (m, 3H) 8.05 (d, J=7.72 Hz, 1H) 9.88 (s, 1H) 15.50 (s, 1H); MS (ESI−) m/z 530 (M−H)−.

Provenance & Evidence