Azepane → HCID 10365527, compound

Participants

Role	Name	HCID	Charge
Reactant	Azepane	HCID 8119	—
Reactant	2-{5-[4-(4-Morpholinylcarbonyl)phenyl]-1-benzofuran-2-yl}ethyl methanesulfonate	HCID 22274531	—
Product	HCID 10365527	HCID 10365527	—

Reaction Steps

The product from Example 23D and azepane were processed as described in Example 1D to provide the titled compound. 1H NMR (300 MHz, CD3OD) δ 7.82 (m, 1H), 7.73 (d, J=8.1, 2H), 7.56 (m, 2H), 7.52 (d, J=8.1 Hz, 2H), 6.77 (s, 1H), 3.3-3.8 (m, 16H), 1.6-2.1 (m, 8H); MS (DCI) m/z 433 (M+H)+;

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US07538138B2
Source dataset	uspto-grants-2009_05
ORD ID	ord-35ef528932ae45a19a38d51ae5f2fa72
Source note	uspto-grants-2009_05