HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodine → (3-Fluorophenyl)(4-hydroxy-3-iodophenyl)methanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodine | HCID 807 | — |
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | (3-Fluorophenyl)(4-hydroxyphenyl)methanone | HCID 11356363 | — |
| Product | (3-Fluorophenyl)(4-hydroxy-3-iodophenyl)methanone | HCID 11325317 | — |
Reaction Steps
The product from Example 69A, potassium iodide and iodine were processed as described in Example 68A to provide the title compound. 1HNMR (300 MHz, CD3OD) δ 6.92 (d, 1H, J=8.9 Hz), 7.31-7.59 (m, 4H), 7.67 (d, 1H, J=8.9 Hz), 8.18 (s, 1H); MS (DCI) m/z 343 (M+H)+, 360 (M+NH4)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07538138B2 |
| Source dataset | uspto-grants-2009_05 |
| ORD ID | ord-c8ec625bb5f2467eb3fdbec987c87d7d |
| Source note | uspto-grants-2009_05 |