HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-p-Chlorophenyl chlorothioformate → 5-[4-(Allyl-methyl-amino)-butoxy]-2,3-dihydro-indole-1-carbothioic acid O-(4-chloro-phenyl)ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-p-Chlorophenyl chlorothioformate | HCID 70306 | — |
| Reactant | Allyl-[4-(2,3-dihydro-1H-indol-5-yloxy)-butyl]-methyl-amine | HCID 21966572 | — |
| Product | 5-[4-(Allyl-methyl-amino)-butoxy]-2,3-dihydro-indole-1-carbothioic acid O-(4-chloro-phenyl)ester | HCID 10159815 | — |
Reaction Steps
In analogy to example 7.8, Allyl-[4-(2,3-dihydro-1H-indol-5-yloxy)-butyl]-methyl-amine and chloro-thioformic acid (4-chloro-phenyl)ester were converted to yield 5-[4-(Allyl-methyl-amino)-butoxy]-2,3-dihydro-indole-1-carbothioic acid O-(4-chloro-phenyl)ester as light grey waxy solid, MS: 431 (MH+, 1Cl).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06706751B2 |
| Source dataset | uspto-grants-2004_03 |
| ORD ID | ord-5f95bf185a894ae39da574258cda160e |
| Source note | uspto-grants-2004_03 |