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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 495156Generated: October 29, 2026

Pyridine → HCID 66593801, compound

https://huagongshe.com/reaction/495156

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPyridineHCID 1049—
Reactant2-Mesitylenesulfonyl chlorideHCID 13046—
ReactantHCID 66593735HCID 66593735—
ProductHCID 66593801HCID 66593801—

Reaction Steps

0.800 g (3.90 mmol) of 2-(2-amino-4-fluorophenyl)-3-methyl-2-cyclopenten-1-one, 0.339 g (4.29 mmol) of pyridine, 0.938 g (4.29 mmol) of 2-mesitylenesulfonyl chloride, and 4 mL of M.C were loaded to a 20 mL vial, and then reacted for 12 hours. The work-up was the same as in Example 7 (1.29 g, 85%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07538239B2
Source datasetuspto-grants-2009_05
ORD IDord-396a3505f94a486f9c14c7be157d4ed7
Source noteuspto-grants-2009_05