HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 66593572, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | 2-Mesitylenesulfonyl chloride | HCID 13046 | — |
| Reactant | HCID 66593482 | HCID 66593482 | — |
| Product | HCID 66593572 | HCID 66593572 | — |
Reaction Steps
0.700 g (3.14 mmol) of 2-(2-amino-5-fluorophenyl)-3-methyl-2-cyclopenten-1-one, 0.273 g (3.45 mmol) of pyridine, 0.754 g (3.45 mmol) of 2-mesitylenesulfonyl chloride, and 3 mL of M.C were loaded to a 20 mL vial, and then reacted for 12 hours. The work-up was the same as in Example 7 (0.760 g, 60%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07538239B2 |
| Source dataset | uspto-grants-2009_05 |
| ORD ID | ord-f908ee54d65d4943afe3bffa08fcaf40 |
| Source note | uspto-grants-2009_05 |