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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 495157Generated: October 30, 2026

Pyridine → HCID 66593572, compound

https://huagongshe.com/reaction/495157

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPyridineHCID 1049—
Reactant2-Mesitylenesulfonyl chlorideHCID 13046—
ReactantHCID 66593482HCID 66593482—
ProductHCID 66593572HCID 66593572—

Reaction Steps

0.700 g (3.14 mmol) of 2-(2-amino-5-fluorophenyl)-3-methyl-2-cyclopenten-1-one, 0.273 g (3.45 mmol) of pyridine, 0.754 g (3.45 mmol) of 2-mesitylenesulfonyl chloride, and 3 mL of M.C were loaded to a 20 mL vial, and then reacted for 12 hours. The work-up was the same as in Example 7 (0.760 g, 60%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07538239B2
Source datasetuspto-grants-2009_05
ORD IDord-f908ee54d65d4943afe3bffa08fcaf40
Source noteuspto-grants-2009_05