HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2-(p-Toluenesulfonyl)aminophenyl)-3-methyl-2-cyclopenten-1-one → 2-(2,5-Dimethylcyclopenta-1,4-dienyl)phenyl(p-toluenesulfonyl)amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2-(p-Toluenesulfonyl)aminophenyl)-3-methyl-2-cyclopenten-1-one | HCID 66593409 | — |
| Reactant | HCID 178418348 | HCID 178418348 | — |
| Product | 2-(2,5-Dimethylcyclopenta-1,4-dienyl)phenyl(p-toluenesulfonyl)amine | HCID 66593708 | — |
Reaction Steps
The same experiment as in Example 17 was carried out, using 1.000 g (2.93 mmol) of 2-(2-(p-toluenesulfonyl)aminophenyl)-3-methyl-2-cyclopenten-1-one and 3.660 ml (5.860 mmol) of MeLi (1.6 M in diethyl ether) (0.617 g, 62%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07538239B2 |
| Source dataset | uspto-grants-2009_05 |
| ORD ID | ord-ce3f199e42eb4b2b8581ea1bc8fabb26 |
| Source note | uspto-grants-2009_05 |