1-Chloro-3-iodopropane → HCID 11075029, compound

HRID 495362Notes

Reaction equation

HRID 495362 reaction equation
[N:1]1[C:6]2[CH:7]=[CH:8][CH:9]=[CH:10][C:5]=2[C:4](=[O:11])[NH:3][N:2]=1.[Cl:12][CH2:13][CH2:14][CH2:15]I>>[Cl:12][CH2:13][CH2:14][CH2:15][N:3]1[C:4](=[O:11])[C:5]2[CH:10]=[CH:9][CH:8]=[CH:7][C:6]=2[N:1]=[N:2]1

Participants

3

Reactant 2

HCID 813631-Chloro-3-iodopropaneHCID 1354087931,2,3-Benzotriazin-4(1H)-one

Product 1

HCID 11075029HCID 11075029, compound

Procedure

3-(3-chloropropyl)-1,2,3-benzotriazin-4(3H)one was prepared according to the general procedure outlined in example 6, step 1. Starting from 1,2,3-benzotriazin-4(3H)one (2 g, 13.6 mmol) and 1-chloro-3-iodopropane (1.6 mL, 14.95 mmol), 1.57 g (52%); yellow solid; m.p. 69° C., MS: 223.9 (M+H)+

Sources & evidence

ORD record
ord-92420d7c6a1f4156b3439ef8bcb758b3
Source dataset
uspto-grants-2005_09
Patent number
US06939870B2

Reaction notes

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