HRID49554

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID3283

Diethyl Ether

C4H10O

HCID21893785

未命名化合物

结构：NS(=O)(=O)c1ccc(C(=O)N[C@H]2CCCC[C@H]2NC(=O)CNC(=O)OCc2ccccc2)cc1

HCID86587037

未命名化合物

PRODUCTS

生成物

结构：Br.NCC(=O)N[C@H]1CCCC[C@H]1NC(=O)c1ccc(S(N)(=O)=O)cc1

HCID68830145

未命名化合物

PROCEDURE

实验过程

The material from above benzyl (cis)-2-[(2-{[4-(aminosulfonyl)benzoyl]amino}cyclohexyl)amino]-2-oxoethylcarbamate (217 mg) was dissolved in 30% HBr/AcOH (5 mL) at rt. After 1 h, Et2O was added and the solid was collected to give N-(cis)-{2-[(aminoacetyl)amino]cyclohexyl}-4-(aminosulfonyl)benzamide hydrogen bromide. MS found: (M+H)+=355.2.

WORKUP

后处理

customthe solid was collected