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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 495667Generated: October 29, 2026

HCID 10908490, compound → HCID 10974237, compound

https://huagongshe.com/reaction/495667

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 10908490HCID 10908490—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 10974237HCID 10974237100%

Reaction Steps

A solution of 1S (430 mg, 0.65 mmol) and 10% Pd/C (80 mg) in methanol (20 ml) was stirred under a hydrogen atmosphere for 30 min. The mixture was filtered through Celite and concentrated to give 413 mg (100%) of unstable glycosylamine 2S which was used without further purification in the next reaction.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06939945B2
Source datasetuspto-grants-2005_09
ORD IDord-d00bf775b4c24f9d9798b513efea8464
Source noteuspto-grants-2005_09