HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10908490, compound → HCID 10974237, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10908490 | HCID 10908490 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 10974237 | HCID 10974237 | 100% |
Reaction Steps
A solution of 1S (430 mg, 0.65 mmol) and 10% Pd/C (80 mg) in methanol (20 ml) was stirred under a hydrogen atmosphere for 30 min. The mixture was filtered through Celite and concentrated to give 413 mg (100%) of unstable glycosylamine 2S which was used without further purification in the next reaction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06939945B2 |
| Source dataset | uspto-grants-2005_09 |
| ORD ID | ord-d00bf775b4c24f9d9798b513efea8464 |
| Source note | uspto-grants-2005_09 |