HRID496084

反应详情

EQUATION

反应方程式

HRID 496084 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A mixture of 3-(p-methoxyphenyl)-1-propylbromide (14 g; 61 mmol) and thiourea (5.1 g; 67 mmol) in ethanol (150 ml) was refluxed for 48 hours. Evaporation of the solvent provided a clear glassy compound, which was dissolved in 50 ml of water and treated with 100 ml of 40% aqueous sodium hydroxide.

WORKUP

后处理

  1. temperaturewas refluxed for 48 hours
  2. customEvaporation of the solvent
  3. customprovided a clear glassy compound, which