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HRID496240

反应详情

EQUATION

反应方程式

HRID 496240 的结构方程式

REACTANTS

反应物

2
结构：CCOC(=O)C(NC(C)=O)C(=O)OCC
HCID14041

Propanedioic acid, 2-(acetylamino)-, 1,3-diethyl ester

C9H15NO5

结构：COc1ccc(C=CC=O)cc1
HCID230995

3-(4-Methoxyphenyl)prop-2-enal

C10H10O2

PRODUCTS

生成物

1
结构：CCOC(=O)C1(C(=O)OCC)C(c2ccc(OC)cc2)CCN1C(C)=O
HCID10021599

未命名化合物

收率 79.5%

PROCEDURE

实验过程

N-Acetyl-2-ethoxycarbonyl-3-(4-methoxyphenyl)proline, ethyl ester (13 g, 72%) was prepared from 4-methoxycinnamaldehyde (Lancaster, 8.1 g, 50 mmol) and diethyl acetamidomalonate (Aldrich, 9.9 g, 45 mmol) by the procedure described by Chung et al (J. Org. Chem. 1990, 55, 270).