HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 9864205, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Dimethylamine, hydrochloride | HCID 10473 | — |
| Reactant | 3-[4-(5,6-Dimethoxy-3-methyl-1,4-benzoquinon-2-ylmethyl)phenyl]propionic acid | HCID 9841061 | — |
| Product | HCID 9864205 | HCID 9864205 | 18% |
Reaction Steps
3-[4-(5,6-dimethoxy-3-methyl-1,4-benzoquinon-2-ylmethyl)phenyl]propionic acid (200 mg, 0.58 mmol) obtained in Example 1 and dimethylamine hydrochloride (62 mg, 0.75 mmol) and triethylamine (76 mg, 0.75 mmol) were used, and a method similar to that described in Example 3 was employed to obtain the title compound (38 mg, 0.10 mmol, yield 18%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06943196B1 |
| Source dataset | uspto-grants-2005_09 |
| ORD ID | ord-b4789d101041408a87850d0e8485e7cf |
| Source note | uspto-grants-2005_09 |