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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 496464Generated: October 30, 2026

Methylamine → HCID 69735306, compound

https://huagongshe.com/reaction/496464

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethylamineHCID 6329—
ReactantHCID 60029928HCID 60029928—
ProductHCID 69735306HCID 69735306—

Reaction Steps

Using the method in Example 172, 3-{[(2-{[(1S)-2-(1H-imidazol-1-yl)-1-phenylethyl]oxy}-5-oxo-5,6,7,8-tetrahydro-1-naphthalenyl)methyl]sulfanyl}benzoic acid (50 mg, 0.10 mmol, 0.20M in DMF) and a saturated solution of methylamine (1.0 ml in DMF) were combined to give 36 mg of the desired compound: Low resolution mass spectrum (LC-MS, APCI) m/z 512 [M+H]+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06943183B2
Source datasetuspto-grants-2005_09
ORD IDord-34838fdb2e674afc88559025af596201
Source noteuspto-grants-2005_09