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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 496536Generated: October 29, 2026

Aluminium lithium hydride → N9-cyclohexylethyl-8-hydroxymethyladenine

https://huagongshe.com/reaction/496536

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAluminium lithium hydrideHCID 21226445—
ReactantN9-cyclohexylethyl-8-methoxycarbonyladenineHCID 54390366—
SolventTetrahydrofuranHCID 8028—
ProductN9-cyclohexylethyl-8-hydroxymethyladenineHCID 53681681—

Reaction Steps

A solution of N9-cyclohexylethyl-8-methoxycarbonyladenine (1 mmol) in tetrahydrofuran was treated with lithium aluminum hydride (1 mmol) at 0° C. for 1 h. Extraction and chromatography give N9-cyclohexylethyl-8-hydroxymethyladenine as a white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06946115B2
Source datasetuspto-grants-2005_09
ORD IDord-a33f8998e12a43c8aff7cfdb8a963059
Source noteuspto-grants-2005_09