HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Oxalate → Ethyl oxo(1,3-thiazol-2-yl)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Oxalate | HCID 7268 | — |
| Reactant | Thiazole | HCID 9256 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Solvent | Hexane | HCID 8058 | — |
| Solvent | Cyclohexane | HCID 8078 | — |
| Product | Ethyl oxo(1,3-thiazol-2-yl)acetate | HCID 54775347 | — |
Reaction Steps
Prepared from thiazole and diethyl oxalate using Method KE-A. In this case the temperature was held at −35° C. and n-butyllithium in hexane was used in place of sec-butyllithium in cyclohexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06946467B2 |
| Source dataset | uspto-grants-2005_09 |
| ORD ID | ord-b6baadba1bf845dbb7fcd861599d38de |
| Source note | uspto-grants-2005_09 |