HCID 16050020, compound → HCID 22321866, compound

Participants

Reaction Steps

A mixture of compound 76(9.4 g), 10% Pd/C (0.94 g) and ethyl acetate (1 L) was stirred under an hydrogen atmosphere at 1 bar pressure for 16 hours. The mixture was filtered through a pad of Celite and the filtrate evaporated under reduced pressure to give methyl 2-phenethyl-5-aminobenzoate (compound 77) as an oil(8.5 g).

Provenance & Evidence