HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 496644Generated: October 30, 2026
Potassium Carbonate → HCID 85876215, compound
https://huagongshe.com/reaction/496644
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Methyl bromoacetate | HCID 60984 | — |
| Reactant | 2,6-Dichloro-4-hydroxybenzaldehyde | HCID 528382 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 85876215 | HCID 85876215 | — |
Reaction Steps
A mixture of 382 mg (2.0 mmol) A1, 337 mg (2.2 mmol) methyl bromoacetate and 387 mg (2.8 mmol) potassium carbonate in 6 ml dry acetone were stirred for 2 h at 60° C. After filtration and removal of the solvent the residue was purified by column chromatography on SiGel (hexane/ethyl acetate 4:1). Yield: 508 mg (97%) A4, colorless solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06946471B2 |
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| Source dataset | uspto-grants-2005_09 |
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| ORD ID | ord-0936ef6cfe5f49ec86935780dbb2f9d2 |
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| Source note | uspto-grants-2005_09 |
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