HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Benzyloxy)-N-methoxy-N-methylbenzamide → 3-hydroxy-N-methoxy-N-methylbenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Benzyloxy)-N-methoxy-N-methylbenzamide | HCID 21865361 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 3-hydroxy-N-methoxy-N-methylbenzamide | HCID 21865376 | 98.4% |
Reaction Steps
To a solution of 100 g (0.37 mol) B4 in 750 ml tetrahydrofurane 10 g Pd/C (10%) were added and the mixture was hydrogenated at atmospheric pressure for 2 hours. The catalyst was filtered off and the filtrate was evaporated to yield 66.0 g B5 (98%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06946471B2 |
| Source dataset | uspto-grants-2005_09 |
| ORD ID | ord-67612ae4688c4a11b5f0b7ed85915b04 |
| Source note | uspto-grants-2005_09 |