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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 496742Generated: October 26, 2026

N,N'-bis-(2-amino-ethyl)-N,N'-dimethyl-propane-1,3-diamine → 3-chloro-6-{2-[(3-{[2-(3-chloro-7-oxo-7H-5,9-diaza-benzo[c]fluoren-6-ylamino)-ethyl]-methyl-amino}-propyl)-methyl-amino]-ethylamino}-5,9-diaza-benzo[c]fluoren-7-one

https://huagongshe.com/reaction/496742

Reaction equation

Participants

RoleNameHCIDCharge
ReactantN,N'-bis-(2-amino-ethyl)-N,N'-dimethyl-propane-1,3-diamineHCID 10607670—
Reactant3-Chloro-6-(toluene-4-sulfonylmethyl)-5,9-diaza-benzo[c]fluoren-7-oneHCID 22322101—
Product3-chloro-6-{2-[(3-{[2-(3-chloro-7-oxo-7H-5,9-diaza-benzo[c]fluoren-6-ylamino)-ethyl]-methyl-amino}-propyl)-methyl-amino]-ethylamino}-5,9-diaza-benzo[c]fluoren-7-oneHCID 10259294—

Reaction Steps

In a similar manner to Example 4, this compound was obtained starting from 3-chloro-6-(toluene-4-sulfonylmethyl)-5,9-diaza-benzo[c]fluoren-7-one (the compound of Reference Example 7c-2) and N,N′-bis-(2-amino-ethyl)-N,N′-dimethyl-propane-1,3-diamine. The desired product was obtained as a reddish powder.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06946472B2
Source datasetuspto-grants-2005_09
ORD IDord-45975a98ad844542a944ac433e3eeb54
Source noteuspto-grants-2005_09