化工社化工社 化学情報印刷レポート · 研究参考用
Hydrochloric Acid → CF3(CF2)7CH2CH2Cl
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Aluminum iodide | HCID 82222 | — |
| 反応物 | 1H,1H,2H-Perfluoro-1-decene | HCID 88990 | — |
| 生成物 | CF3(CF2)7CH2CH2Cl | HCID 85612084 | — |
反応手順
The same process as in Example 1 was conducted except that 41 g of CF3(CF2)7CH═CH2, 12 g of CaSO4/C (25/75 mass %) instead of AlI3, and 3.4 g of hydrogen chloride gas instead of 11 g of hydrogen iodide gas were used. CF3(CF2)7CH2CH2Cl was produced at a conversion rate of 1.7% and at a selectivity of 100%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06946582B2 |
| 出典データセット | uspto-grants-2005_09 |
| ORD ID | ord-5c1d5956ba7047cea384543dee7432df |
| 出典メモ | uspto-grants-2005_09 |