HCID 12072042, compound → HCID 12072043, compound

Participants

Reaction Steps

4-[6-Chloro-1-(2-morpholin-4-yl-ethyl)-1H-indol-3-yl]-piperidine-1-carboxylic acid tert-butyl ester (2.6 g, 5.81 mmol) was set stirring in 1:1 TFA/CH2Cl2. After 45 min the mixture was evaporated and the golden oil brought up in Et2O. A solid formed and was filtered, washed with Et2O and air dried to give 2.5 g (95%) of a white solid. MS (electrospray): exact mass calculated for C19H26ClN3O, 347.18; m/z found, 348.2 [M++H].

Provenance & Evidence