2-Fluoroaniline → HCID 86588317, compound

HRID 497401Notes

Reaction equation

HRID 497401 reaction equation
[F:1][C:2]1[CH:8]=[CH:7][CH:6]=[CH:5][C:3]=1[NH2:4].C([O:11][C:12]([C:14]1[C:23]2[C:22]3[N:24]([CH3:27])[N:25]=[CH:26][C:21]=3[CH2:20][CH2:19][CH2:18][C:17]=2[NH:16][CH:15]=1)=O)C>>[F:1][C:2]1[CH:8]=[CH:7][CH:6]=[CH:5][C:3]=1[NH:4][C:12]([C:14]1[C:23]2[C:22]3[N:24]([CH3:27])[NH:25][CH2:26][C:21]=3[CH2:20][CH2:19][CH2:18][C:17]=2[NH:16][CH:15]=1)=[O:11]

Participants

3

Reactant 2

HCID 95842-FluoroanilineHCID 136079968HCID 136079968, compound

Product 1

HCID 86588317HCID 86588317, compound

Procedure

The title compound is prepared according to Example 9 using 2-fluoroaniline and 1-methyl-4,5,6,7-tetrahydro-1H-1,2,7-triaza-cyclopenta[e]azulene-9-carboxylic acid ethyl ester. Electrospray mass spectrum: m/z 325 [M+1].

Sources & evidence

ORD record
ord-bf84e71129ce41859aacee61392bad87
Source dataset
uspto-grants-2005_09
Patent number
US06949562B2

Reaction notes

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