HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Decanoate → Decanohydrazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Decanoate | HCID 8050 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Decanohydrazide | HCID 98597 | 94% |
Reaction Steps
17.5 g of decanoic acid methyl ester is dissolved in 1 l of absolute ethanol and mixed with 350 ml of hydrazine hydrate. It is refluxed for 3 hours and then stirred overnight at room temperature. The solution is concentrated by evaporation to about 300 ml and allowed to stand until the product is crystallized out. After it is filtered off and dried, 16.6 g (=94% of theory) of decanoic acid hydrazide is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06709693B1 |
| Source dataset | uspto-grants-2004_03 |
| ORD ID | ord-d63e462b8fd14c8bbc6a3c4b6aae5b72 |
| Source note | uspto-grants-2004_03 |