Hydrochloric Acid → HCID 23393475, compound

Participants

Reaction Steps

1.76 ml of HCl (1N) was added slowly to a solution of 1.63 g (4.53 mmol) of 1,5-dimethyl-1-[3-(2-phenyl-1,3-dioxolan-2-yl)propyl]-4-hexenyl acetate obtained under d) in 30 ml of THF. The reaction mixture was stirred at 40° or 4 h, cooled down to room temperature, extracted with ether, washed with a saturated solution of NaCl (3×), dried (Na2SO4), filtered and concentrated. Column chromatography (SiO2, heptane/ether 4:1) yielded 1.34 g (94%) of a slightly yellow oil.

Provenance & Evidence