HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 24720925, compound → tert-butyl N-(2-amino-4-(trifluoromethyl)phenyl)carbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 24720925 | HCID 24720925 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | tert-butyl N-(2-amino-4-(trifluoromethyl)phenyl)carbamate | HCID 24689211 | — |
Reaction Steps
The title compound was prepared from (2-nitro-4-trifluoromethyl-phenyl)-carbamic acid tert-butyl ester (Example A4) (30.0 g, 98 mmol) by hydrogenation with 10% Pd/C according to the general procedure J (method a). Obtained as a light yellow solid (26.5 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06949542B2 |
| Source dataset | uspto-grants-2005_09 |
| ORD ID | ord-5de8fb443640430ebc5c94615725dcf3 |
| Source note | uspto-grants-2005_09 |