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HRID 498204作成日：2026年10月25日

[5-(Methyl-propyl-amino)-2-nitro-4-trifluoromethyl-phenyl]-carbamic acid tert-butyl ester → Carbamic acid,[2-amino-5-(methylpropylamino)-4-(trifluoromethyl)phenyl]-,1,1-dimethylethyl ester

https://huagongshe.com/reaction/498204

反応式

関与物質

役割名称HCID仕込み量
反応物[5-(Methyl-propyl-amino)-2-nitro-4-trifluoromethyl-phenyl]-carbamic acid tert-butyl esterHCID 69487144—
触媒PalladiumHCID 23938—
生成物Carbamic acid,[2-amino-5-(methylpropylamino)-4-(trifluoromethyl)phenyl]-,1,1-dimethylethyl esterHCID 69486655—

反応手順

The title compound was prepared from [5-(methyl-propyl-amino)-2-nitro-4-trifluoromethyl-phenyl]-carbamic acid tert-butyl ester (Example C5) (3.78 g, 10.0 mmol) by hydrogenation with 10% Pd/C according to the general procedure J (method a). Obtained as a red oil (3.40 g, 98%).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US06949542B2
出典データセットuspto-grants-2005_09
ORD IDord-9f8e75c493db45df88d0c26740e94504
出典メモuspto-grants-2005_09