HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stannous chloride dihydrate → HCID 69489430, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stannous chloride dihydrate | HCID 61436 | — |
| Reactant | Carbamic acid, (5-chloro-4-methyl-2-nitrophenyl)-, 1,1-dimethylethyl ester | HCID 69486680 | — |
| Product | HCID 69489430 | HCID 69489430 | — |
Reaction Steps
(2-Amino-5-chloro-4-methyl-phenyl)-carbamic acid tert-butyl ester was prepared from (5-chloro-4-methyl-2-nitro-phenyl)-carbamic acid tert-butyl ester (Example A16) (11.9 g, 41.4 mmol) by reduction with SnCl2.2H2O according to the general procedure J (method b). Obtained as a yellow solid (9.25 g, 87%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06949542B2 |
| Source dataset | uspto-grants-2005_09 |
| ORD ID | ord-40982624714c45139eb27aefd262491a |
| Source note | uspto-grants-2005_09 |