HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69489095, compound → HCID 69489849, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69489095 | HCID 69489095 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 69489849 | HCID 69489849 | — |
Reaction Steps
The title compound was prepared from [2-nitro-4-(2,2,2-trifluoro-ethoxy)-phenyl]-carbamic acid tert-butyl ester (Example A24) (3.65 g, 11 mmol) by hydrogenation with 10% Pd/C according to the general procedure J (method a). Obtained as a light brown solid (3.16 g, 94%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06949542B2 |
| Source dataset | uspto-grants-2005_09 |
| ORD ID | ord-c594c50bade746d0abed259e383fe3ca |
| Source note | uspto-grants-2005_09 |