HuagongsheHuagongshe Chemistry Print Report · For research reference only
(5-Fluoro-2-nitro-4-trifluoromethyl-phenyl)-carbamic acid tert-butyl ester → HCID 69489617, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (5-Fluoro-2-nitro-4-trifluoromethyl-phenyl)-carbamic acid tert-butyl ester | HCID 12048024 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 69489617 | HCID 69489617 | — |
Reaction Steps
The title compound was prepared from (5-fluoro-2-nitro-4-trifluoromethyl-phenyl)-carbamic acid tert-butyl ester (Example A2) (3.34 g, 10.3 mmol) by hydrogenation with 10% Pd/C according to the general procedure J (method a). Obtained as a yellow solid (2.93 g, 97%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06949542B2 |
| Source dataset | uspto-grants-2005_09 |
| ORD ID | ord-07296e138c7b44deb813db2ac79e578b |
| Source note | uspto-grants-2005_09 |