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Methyl 3-(3-pyridinyl)benzoate → 3-Oxo-3-(3-pyridin-3-yl-phenyl)-propionic acid tert-butyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl 3-(3-pyridinyl)benzoate | HCID 4133188 | — |
| 反応物 | Lithium Tert-butyl Acetate | HCID 86586795 | — |
| 生成物 | 3-Oxo-3-(3-pyridin-3-yl-phenyl)-propionic acid tert-butyl ester | HCID 11266473 | — |
反応手順
The title compound was prepared from 3-pyridin-3-yl-benzoic acid methyl ester [CAS-No. 79601-27-7] (1.00 g, 4.69 mmol) by treatment with lithium tert-butyl acetate according to general procedure K (method b). Obtained as an orange oil (673 mg).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06949542B2 |
| 出典データセット | uspto-grants-2005_09 |
| ORD ID | ord-587a230e430241afb4926e8958425456 |
| 出典メモ | uspto-grants-2005_09 |