HuagongsheHuagongshe Chemistry Print Report · For research reference only
N1-(tert-Butoxycarbonyl)-4-fluoro-1,2-phenylenediamine → HCID 86589281, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N1-(tert-Butoxycarbonyl)-4-fluoro-1,2-phenylenediamine | HCID 24688763 | — |
| Reactant | 3-[3-(2-Methyl-pyridin-4-yl)-phenyl]-3-oxo-propionic acid tert-butyl ester | HCID 69489307 | — |
| Product | HCID 86589281 | HCID 86589281 | 84.1% |
Reaction Steps
The compound was prepared from (2-amino-4-fluoro-phenyl)-carbamic acid tert-butyl ester (Example J2) (226 mg, 1.0 mmol) and 3-[3-(2-methyl-pyridin-4-yl)-phenyl]-3-oxo-propionic acid tert-butyl ester (Example K12) (311 mg, 1.0 mmol) according to the general procedure M. Obtained as an off-white foam (390 mg, 84%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06949542B2 |
| Source dataset | uspto-grants-2005_09 |
| ORD ID | ord-52697756f0094629a88f4656d8b4fc77 |
| Source note | uspto-grants-2005_09 |