HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-[3-(2-Methyl-pyridin-4-yl)-phenyl]-3-oxo-propionic acid tert-butyl ester → HCID 86589348, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-[3-(2-Methyl-pyridin-4-yl)-phenyl]-3-oxo-propionic acid tert-butyl ester | HCID 69489307 | — |
| Reactant | HCID 69489646 | HCID 69489646 | — |
| Product | HCID 86589348 | HCID 86589348 | — |
Reaction Steps
The title compound was prepared from (2-amino-4-chloro-5-ethoxy-phenyl)-carbamic acid tert-butyl ester (Example J25) (215 mg, 0.75 mmol) and 3-[3-(2-methyl-pyridin-4-yl)-phenyl]-3-oxo-propionic acid tert-butyl ester (Example K12) (234 mg, 0.75 mmol) according to the general procedure M. Obtained as an off-white solid (280 mg, 71%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06949542B2 |
| Source dataset | uspto-grants-2005_09 |
| ORD ID | ord-9a5e918400834e228e8b2de1180897b9 |
| Source note | uspto-grants-2005_09 |