HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbamic acid,n-[2-amino-5-ethyl-4-(trifluoromethyl)phenyl]-,1,1-dimethylethyl ester → HCID 86589374, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbamic acid,n-[2-amino-5-ethyl-4-(trifluoromethyl)phenyl]-,1,1-dimethylethyl ester | HCID 69486873 | — |
| Reactant | 3-[3-(2-Cyano-pyridin-4-yl)-phenyl]-3-oxo-propionic acid tert-butyl ester | HCID 69489885 | — |
| Product | HCID 86589374 | HCID 86589374 | — |
Reaction Steps
The title compound was prepared from (2-amino-5-ethyl-4-trifluoromethyl-phenyl)-carbamic acid tert-butyl ester (Example J33) (228 mg, 0.75 mmol) and 3-[3-(2-cyano-pyridin-4-yl)-phenyl]-3-oxo-propionic acid tert-butyl ester (Example K24) (242 mg, 0.75 mmol) according to the general procedure M. Obtained as a light brown solid (308 mg, 74%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06949542B2 |
| Source dataset | uspto-grants-2005_09 |
| ORD ID | ord-87d3605e79454f38a1fd1fc928bcca02 |
| Source note | uspto-grants-2005_09 |