4,5-Dichloro-1,2-phenylenediamine → HCID 22317286, compound

Participants

Reaction Steps

The title compound was prepared from commercially available 4,5-dichloro-1,2-phenylendiamine (133 mg, 0.75 mmol) and 3-[3-(2-ethyl-pyridin-4-yl)-phenyl]-3-oxo-propionic acid tert-butyl ester (Example K20) (244 mg, 0.75 mmol) in xylene (7.5 ml) under reflux conditions for 1.5 h according to the general procedure M. Obtained as a light red solid (236 mg, 77%).

Provenance & Evidence