HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 22317469, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | {5-Ethoxy-2-[3-oxo-3-(3-pyridin-4-yl-phenyl)-propionylamino]-phenyl}-carbamic acid tert-butyl ester | HCID 86589330 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22317469 | HCID 22317469 | — |
Reaction Steps
The title compound was prepared from {5-ethoxy-2-[3-oxo-3-(3-pyridin-4-yl-phenyl)-propionylamino]-phenyl}-carbamic acid tert-butyl ester (Example M145) (193 mg, 0.41 mmol) by treatment with TFA in CH2Cl2 according to the general procedure N. Obtained as a brown solid (105 mg, 72%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06949542B2 |
| Source dataset | uspto-grants-2005_09 |
| ORD ID | ord-b924ecd3c10242aa8aa8ffbc09c73066 |
| Source note | uspto-grants-2005_09 |