HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 22317997, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 86589492 | HCID 86589492 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22317997 | HCID 22317997 | — |
Reaction Steps
The title compound was prepared from (4-chloro-5-methyl-2-{3-oxo-3-[3-(2-trifluoromethyl-pyridin-4-yl)-phenyl]-propionylamino}-phenyl)-carbamic acid tert-butyl ester (Example M244) (0.26 g, 0.47 mmol) by treatment with TFA in CH2Cl2 according to the general procedure N. Obtained as an off-white solid (200 mg, 98%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06949542B2 |
| Source dataset | uspto-grants-2005_09 |
| ORD ID | ord-b1600553963d424d963a07343bea078f |
| Source note | uspto-grants-2005_09 |