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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 498768Generated: October 30, 2026

HCID 69486742, compound → HCID 22317403, compound

https://huagongshe.com/reaction/498768

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 69486742HCID 69486742—
Reactanttert-Butyl (2-amino-4-chloro-5-methylphenyl)carbamateHCID 69486983—
ProductHCID 22317403HCID 22317403—

Reaction Steps

The title compound was prepared from (2-amino-4-chloro-5-methyl-phenyl)-carbamic acid tert-butyl ester (Example J22) (67 mg, 0.26 mmol) and 3-(2′-methyl-[2,4′]bipyri-dinyl-4-yl)-3-oxo-propionic acid tert-butyl ester (Example K59) (81 mg, 0.26 mmol) according to the general procedure M and subsequent treatment of the crude product according to the general procedure N. Obtained as a light yellow solid (69 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06949542B2
Source datasetuspto-grants-2005_09
ORD IDord-ecb88db7b7514d2a8b0cd6a4e6d94d9f
Source noteuspto-grants-2005_09