HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 499270Generated: October 29, 2026
Pyridine-2-carbonitrile → HCID 59750340, compound
https://huagongshe.com/reaction/499270
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Pyridine-2-carbonitrile | HCID 7522 | — |
| Reactant | 2-Mercapto-3-methoxybenzoic acid | HCID 16655610 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 59750340 | HCID 59750340 | 28% |
Reaction Steps
A mixture of 3-methoxy-2-mercaptobenzoic acid (1.84 g, 10.0 mmol), 2-cyanopyridine (1.05 g, 10.2 mmol) and pyridine (30.0 ml) was refluxed at 135° C. for 18 hrs as described in Example 9. The mixture was concentrated. The obtained crystals were recrystallized from ethanol to give the titled compound (0.75 g, 28%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07767665B2 |
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| Source dataset | uspto-grants-2010_08 |
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| ORD ID | ord-aa6d7a7476f4414b9e58fbba8e9dd439 |
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| Source note | uspto-grants-2010_08 |
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