HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 22939353, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Benzoic acid, 2-mercapto-, methyl ester | HCID 21009 | — |
| Reactant | 6-(Benzyloxy)picolinonitrile | HCID 11052904 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 22939353 | HCID 22939353 | 26% |
Reaction Steps
A mixture of methyl thiosalicylate (0.40 g, 2.4 mmol), 2-benzyloxy-6-cyanopyridine (0.50 g, 2.4 mmol), triethylamine (0.50 ml, 3.6 mmol) and toluene (30 ml) was refluxed for 48 hrs as described in Example 1. The reaction mixture was concentrated under reduced pressure and recrystallized from ethanol to give the titled compound (0.21 g, 26%) as crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07767665B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-3f8af14abe554bdabd5db219896090a0 |
| Source note | uspto-grants-2010_08 |