HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 9012670, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Cyanophenol | HCID 13019 | — |
| Reactant | Methyl 3-(bromomethyl)benzoate | HCID 517981 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 9012670 | HCID 9012670 | — |
Reaction Steps
500 mg (2.18 mmol) of methyl 3-bromomethylbenzoate, 437 mg (2.40 mmol) of 4-hydroxybenzonitrile and 600 mg of potassium carbonate were stirred in dimethylformamide at room temperature for 1.5 hours. The reaction mixture was filtered through Celite, then treated by an ordinary method and purified by the silica gel column chromatography to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06710056B2 |
| Source dataset | uspto-grants-2004_03 |
| ORD ID | ord-ed85861d1c884e0d93967395beef5c5a |
| Source note | uspto-grants-2004_03 |