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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 49937Generated: October 29, 2026

Potassium Carbonate → HCID 9012670, compound

https://huagongshe.com/reaction/49937

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
Reactant4-CyanophenolHCID 13019—
ReactantMethyl 3-(bromomethyl)benzoateHCID 517981—
SolventDimethylformamideHCID 6228—
ProductHCID 9012670HCID 9012670—

Reaction Steps

500 mg (2.18 mmol) of methyl 3-bromomethylbenzoate, 437 mg (2.40 mmol) of 4-hydroxybenzonitrile and 600 mg of potassium carbonate were stirred in dimethylformamide at room temperature for 1.5 hours. The reaction mixture was filtered through Celite, then treated by an ordinary method and purified by the silica gel column chromatography to obtain the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06710056B2
Source datasetuspto-grants-2004_03
ORD IDord-ed85861d1c884e0d93967395beef5c5a
Source noteuspto-grants-2004_03